Table 2. Integrated Hydrogen Areas from the IINS Spectra in Order of Increasing Average Primary Particle Sizea.
| Catalyst (sample no.) | Morphologyb | DN/nmc | Relative aread |
|---|---|---|---|
| Pd(20%)/carbon black (2) | agg | 2.40 | 1.31 |
| Pd(20%)/activated carbon (1) | prim | 3.58 | 1.00 |
| Pd(20%)/carbon black 300 °C (3) | agg/prim | 6.73 | 1.65 |
| Pd(20%)/carbon black 400 °C (4) | prim | 7.74 | 1.30 |
Reproduced with permission from ref (129) under a Creative Commons Attribution 3.0 Unported License (CC-BY).
Morphological differences according to TEM: agg = mostly aggregates, prim = mostly isolated primary particles.
Average particle size from statistical determination by TEM.