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. 2023 Jun 7;415(19):4731–4740. doi: 10.1007/s00216-023-04766-9

Table 2.

Composition of the solvent system n-hexane/ethanol/methanol/water (34:11:12:2, v/v/v/v) in percent (± 3% standard deviation), determined by GC/FID and Karl Fischer titration

n-Hexane Ethanol Methanol Water
Upper phase 95.0 3.2 1.6 0.2
Lower phase 20.1 34.8 39.1 6.0