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. 2023 Jun 20;25(27):4980–4984. doi: 10.1021/acs.orglett.3c01554

Scheme 2. Solid Phase Peptide Synthesis of a 4-Thio-ADP-Ribosylated H2B Peptide.

Scheme 2

Abbreviations: DBU, 1,8-diazabicyclo[5.4.0]undec-7-ene; ETT, 5-ethylthio-1H-tetrazole; Mtt, 4-methytrityl; SPPS, solid phase peptide synthesis; TBAF, tetra-n-butylammonium fluoride; TFA, trifluoroacetic acid.