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. 2023 Jul 19;13(31):21673–21684. doi: 10.1039/d3ra03441k

Study of matrix effect in the juice samples spiked at different concentrations. All samples were diluted with deionized water at a ratio of 1 : 1.

Analytes Mean relative recovery ± standard deviation (n = 3)
Fresh apple juice Peach juice Pineapple juice Apple juice Mango juice Fresh orange juice
All samples were spiked with each analyte at a concentration of 30 μg L−1
Chlorpyrifos 95 ± 2 97 ± 2 94 ± 3 97 ± 2 92 ± 2 96 ± 2
Haloxyfop-R-methyl 97 ± 2 93 ± 3 96 ± 3 92 ± 2 91 ± 2 91 ± 2
Oxadiazon 96 ± 3 90 ± 3 90 ± 3 90 ± 4 93 ± 4 92 ± 2
Diniconazole 91 ± 2 92 ± 4 91 ± 3 91 ± 3 90 ± 3 97 ± 2
Clodinafop-propargyl 94 ± 3 88 ± 4 93 ± 2 92 ± 2 95 ± 2 96 ± 2
Fenpropathrin 93 ± 2 98 ± 4 94 ± 3 93 ± 3 92 ± 4 93 ± 2
Fenaxaprop-P-ethyl 90 ± 4 94 ± 3 92 ± 4 95 ± 3 89 ± 3 90 ± 3
All samples were spiked with each analyte at a concentration of 60 μg L−1
Chlorpyrifos 95 ± 3 93 ± 2 94 ± 2 97 ± 3 92 ± 3 96 ± 2
Haloxyfop-R-methyl 90 ± 4 90 ± 3 91 ± 2 92 ± 2 89 ± 2 91 ± 3
Oxadiazon 91 ± 2 96 ± 2 92 ± 2 87 ± 3 93 ± 2 89 ± 3
Diniconazole 93 ± 3 92 ± 3 96 ± 2 95 ± 2 85 ± 3 98 ± 3
Clodinafop-propargyl 92 ± 3 87 ± 4 89 ± 2 89 ± 3 94 ± 4 99 ± 2
Fenpropathrin 94 ± 4 98 ± 3 93 ± 2 93 ± 3 92 ± 4 94 ± 2
Fenaxaprop-P-ethyl 97 ± 3 89 ± 2 95 ± 2 91 ± 2 90 ± 3 97 ± 3