Study of matrix effect in the juice samples spiked at different concentrations. All samples were diluted with deionized water at a ratio of 1 : 1.
| Analytes | Mean relative recovery ± standard deviation (n = 3) | |||||
|---|---|---|---|---|---|---|
| Fresh apple juice | Peach juice | Pineapple juice | Apple juice | Mango juice | Fresh orange juice | |
| All samples were spiked with each analyte at a concentration of 30 μg L−1 | ||||||
| Chlorpyrifos | 95 ± 2 | 97 ± 2 | 94 ± 3 | 97 ± 2 | 92 ± 2 | 96 ± 2 |
| Haloxyfop-R-methyl | 97 ± 2 | 93 ± 3 | 96 ± 3 | 92 ± 2 | 91 ± 2 | 91 ± 2 |
| Oxadiazon | 96 ± 3 | 90 ± 3 | 90 ± 3 | 90 ± 4 | 93 ± 4 | 92 ± 2 |
| Diniconazole | 91 ± 2 | 92 ± 4 | 91 ± 3 | 91 ± 3 | 90 ± 3 | 97 ± 2 |
| Clodinafop-propargyl | 94 ± 3 | 88 ± 4 | 93 ± 2 | 92 ± 2 | 95 ± 2 | 96 ± 2 |
| Fenpropathrin | 93 ± 2 | 98 ± 4 | 94 ± 3 | 93 ± 3 | 92 ± 4 | 93 ± 2 |
| Fenaxaprop-P-ethyl | 90 ± 4 | 94 ± 3 | 92 ± 4 | 95 ± 3 | 89 ± 3 | 90 ± 3 |
| All samples were spiked with each analyte at a concentration of 60 μg L−1 | ||||||
| Chlorpyrifos | 95 ± 3 | 93 ± 2 | 94 ± 2 | 97 ± 3 | 92 ± 3 | 96 ± 2 |
| Haloxyfop-R-methyl | 90 ± 4 | 90 ± 3 | 91 ± 2 | 92 ± 2 | 89 ± 2 | 91 ± 3 |
| Oxadiazon | 91 ± 2 | 96 ± 2 | 92 ± 2 | 87 ± 3 | 93 ± 2 | 89 ± 3 |
| Diniconazole | 93 ± 3 | 92 ± 3 | 96 ± 2 | 95 ± 2 | 85 ± 3 | 98 ± 3 |
| Clodinafop-propargyl | 92 ± 3 | 87 ± 4 | 89 ± 2 | 89 ± 3 | 94 ± 4 | 99 ± 2 |
| Fenpropathrin | 94 ± 4 | 98 ± 3 | 93 ± 2 | 93 ± 3 | 92 ± 4 | 94 ± 2 |
| Fenaxaprop-P-ethyl | 97 ± 3 | 89 ± 2 | 95 ± 2 | 91 ± 2 | 90 ± 3 | 97 ± 3 |