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(A) Comparison of CO/H2 and CO partial current densities after 3 h electrolysis of 0.1 mM [Ni(cyclam)]2+ in 0.5 M NaCl (aq) where EC [tC] = −1.6 VAg/AgCl [5 s]; tA= 0.2 s with changing EA. (B) Schematic illustrating the proposed mechanism of how pulsed electrolysis can reduce catalyst degradation.
