TABLE 1.

Gradient time program for flash separation.

Time [h:min:s]	Phosphate buffer [%]	Acetonitrile [%]
0:00:00	30	70
0:07:00	30	70
0:17:00	38	62
0:20:00	38	62
0:25:00	40	60
1:30:00	40	60
2:10:00	42	58
2:10:00	42	58
2:25:00	55	45