Table 1. 1H and 13C NMR Data of Compound 10 (CDCl3; 500 MHz for 1H and 126 MHz for 13C NMR; δ in ppm).
| positiona | δC, type | δH (J in Hz)b |
|---|---|---|
| 1 | 129.1, C | |
| 2, 6 | 127.9, CH | 7.36, d (8.5) |
| 3, 5 | 114.9, CH | 6.93 d (8.5) |
| 4 | 158.7 C | |
| 7 | 134.1, CH | 6.67 d (15.9) |
| 8 | 121.0, CH | 6.25 |
| 9 | 65.4 CH2 | 4.86 dd (6.1, 0.9) |
| 1′ | 134.4 C | |
| 2′, 6′ | 128.1 CH | 7.54 m |
| 3′, 5′ | 128.9 CH | 7.39 |
| 4′ | 130.3 CH | 7.39 |
| 7′ | 145.0 CH | 7.74 d (16.2) |
| 8′ | 118.0 CH | 6.49 d (15.9) |
| 9′ | 166.8 C | |
| 1″ | 129.1 C | |
| 2″, 6″ | 128.0 CH | 7.31 d (8.5) |
| 3″, 5″ | 1115.4 CH | 6.80 d (8.5) |
| 4″ | 155.4 C | |
| 7″ | 132.9 CH | 6.67 d (15.9) |
| 8″ | 121.9 CH | 6.28 |
| 9″ | 68.8 CH2 | 4.69 dd (6.1, 1.2) |