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. 2023 Jul 19;12(7):1453. doi: 10.3390/antiox12071453

Table 2.

Effects of extrusion on the terpene and terpenoid content.

Food Matrix Experiment Conditions Terpenes Ref.
Extrusion Parameters Sample Type Amount
Corn, carrot powder, ascorbic acid
  • -

    single-screw extruder, temperature profiles of 135/170/170 °C, 4:1 compression ratio screw, screw speed of 100 rpm, feed rate of 15 rpm.

  • -

    control

  • -

    4% carrot powder

  • -

    6% carrot powder

  • -

    8% carrot powder

9-cis-β-Carotene
(mg EβC/kg)
0.00 to 0.00 =
0.52 to 0.00 ↓
0.44 to 0.44 =
0.74 to 0.79 ↑
[84]
  • -

    control

  • -

    4% carrot powder

  • -

    6% carrot powder

  • -

    8% carrot powder

Lutein
(mg/kg)
32.80 to 87.70 ↑
21.70 to 36.70 ↑
21.20 to 52.00 ↑
16.70 to 39.90 ↑
  • -

    control

  • -

    4% carrot powder

  • -

    6% carrot powder

  • -

    8% carrot powder

Zeaxanthin
(mg/kg)
32.80 to 42.90 ↑
25.30 to 29.00 ↑
19.10 to 24.40 ↑
25.90 to 25.80 ↓
Quinoa flour
  • -

    moisture adjusted at 18%;

  • -

    twin-screw extruder, temperature of 75 °C, 105 °C, and 135 °C, screw rotation speed of 251–253 rpm, three nozzles of 2.6 mm diameter.

  • -

    quinoa flour

Total carotenoids
(mg β-carotene/g d.w.)
11.33 to 8.39 ↓ [67]
Corn with pea and rosehip
  • -

    single-screw laboratory extruder, barrel diameter of 19 mm, 3:1 compression ratio, dosing speed of 18 rpm, feed rate of 3.51 kg/h, rotation speed of 150 rpm, temperatures of barrel sections of 25/70/170/175 °C, nozzle diameter of 3 mm.

  • -

    control (corn flour)

  • -

    10% rosehip;

  • -

    10% rosehip + pea protein

Total carotenoids
(mg β-carotene/100 g d.w.)
3.75 to 2.11 ↓
43.74 to 7.85 ↓
22.73 to 5.76 ↓
[85]
Corn with carrot pomace
  • -

    co-rotating twin-screw extruder, screw diameter of 20 mm, 15% moisture of corn-carrot pomace mix, 20 mm 4 individual heating zones (50/100/140/140 °C), die with a diameter of 4.0 mm.

  • -

    5% carrot pomace

  • -

    10% carrot pomace

  • -

    15% carrot pomace

β-carotene
(mg/100 g)
0.34 to 0.26 ↓
0.53 to 0.29 ↓
0.96 to 0.34 ↓
[99]
Maize
  • -

    single-screw extruder, zones temperatures of 60/70/80/90 °C, die diameter of 5 mm, screw speed of 60 rpm.

  • -

    20% moisture

  • -

    25% moisture

  • -

    30% moisture

Lutein
(μg/100 g)
94.30 to 39.50 ↓
94.30 to 43.0 ↓
94.30 to 34.0 ↓
[65]
  • -

    20% moisture

  • -

    25% moisture

  • -

    30% moisture

Zeaxanthin
(μg/100 g)
189.70 to 61.0 ↓
189.70 to 54.00 ↓
189.70 to 47.70 ↓
  • -

    20% moisture

  • -

    25% moisture

  • -

    30% moisture

β-carotene
(μg/100 g)
15.90 to 11.30 ↓
15.90 to 8.30 ↓
15.90 to 6.40 ↓
  • -

    20% moisture

  • -

    25% moisture

  • -

    30% moisture

Campesterol
(mg/100 g)
23.30 to 21.20 ↓
23.30 to 22.40 ↓
23.30 to 26.30 ↓
  • -

    20% moisture

  • -

    25% moisture

  • -

    30% moisture

Stigmasterol
(mg/100 g)
13.70 to 12.90 ↓
13.70 to 14.00 ↓
13.70 to 15.60 ↓
  • -

    20% moisture

  • -

    25% moisture

  • -

    30% moisture

β-sitosterol
(mg/100 g)
140.30 to 121.60 ↓
140.30 to 127.70 ↓
140.30 to 145.90 ↓
Corn grits with carrot
  • -

    twin-screw extruder, die diameter of 3 mm, feeding rate of 36 ± 1 g/min, temperature profile of 80/90/100/130//120 °C, screw speed of 125 rpm

  • -

    corn + carrot pulp

β-carotene (μg/g d.w.) 11.13 to 4.23 ↓ [88]
Lutein (μg/g d.w.) 2.66 to 1.91 ↓
Intermediate wheatgrass
  • -

    corotating twin-screw extruder, screw diameter of 20 mm, temperature profile of 50/80/120/150/150/150 °C, screw speed of 200 rpm.

  • -

    intermediate wheatgrass

Lutein (μg/g flour) 14.53 to 3.52 ↓ [68]
Zeaxanthin (μg/g flour) 3.39 to 1.16 ↓
Maize
  • -

    co-rotating twin-screw extruder, barrel temperature of 140.7 °C, feed moisture of 20%, screw speed of 400 rpm, 5 mm die diameter

  • -

    PVAH 79–100 1

  • -

    PVAH 1–26 1

  • -

    PVAH 27–49 1

  • -

    PVAH 50–75 1

β-Carotene
(mg/kg)
0.83 to 0.49 ↓
0.83 to 0.41 ↓
0.86 to 0.47 ↓
0.88 to 0.49 ↓
[100]
  • -

    PVAH 79–100 1

  • -

    PVAH 1–26 1

  • -

    PVAH 27–49 1

  • -

    PVAH 50–75 1

9-cis-β-Carotene (mg/kg) 0.53 to 0.36 ↓
0.52 to 0.38 ↓
0.56 to 0.41 ↓
0.57 to 0.36 ↓
  • -

    PVAH 79–100 1

  • -

    PVAH 1–26 1

  • -

    PVAH 27–49 1

  • -

    PVAH 50–75 1

13-cis-β-Carotene (mg/kg) 0.47 to 0.33 ↓
0.47 to 0.31 ↓
0.47 to 0.32 ↓
0.47 to 0.33 ↓
  • -

    PVAH 79–100 1

  • -

    PVAH 1–26 1PVAH 27–49 1

  • -

    PVAH 50–75 1

β-Cryptoxanthin
(mg/kg)
1.17 to 0.39 ↓
1.53 to 0.39 ↓
1.15 to 0.39 ↓
1.21 to 1.38 ↓
Corn with peach palm
  • -

    twin-screw extruder, temperature profile of 30/50/80/90/90/100/100/100/130/130 °C, screw speed of 400 rpm, die diameter of 8 mm, flow rate of 8 kg/h, moisture of 16 g/100 g

  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

Lutein
(μg/g d.w.)
0.78 to 1.72 ↑
0.55 to 1.23 ↑
1.25 to 0.80 ↓
0.60 to 1.34 ↑
0.55 to 0.58 ↑
[101]
  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

Zeaxanthin
(μg/g d.w.)
1.11 to 3.39 ↑
0.57 to 1.18 ↑
1.32 to 1.64 ↑
1.24 to 1.52 ↑
0.73 to 0.94 ↑
  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

β-cryptoxanthin
(μg/g d.w.)
0.42 to 0.78 ↑
0.50 to 0.52 ↑
0.36 to 0.47 ↑
0.45 to 0.58 ↑
0.22 to 0.47 ↑
  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

α-carotene
(μg/g d.w.)
0.02 to 0.00 ↓
0.10 to 0.09 ↓
0.15 to 0.12 ↓
0.15 to 0.14 ↓
0.12 to 0.25 ↑
  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

β-carotene
(μg/g d.w.)
0.44 to 0.68 ↑
1.33 to 0.84 ↓
1.62 to 1.28 ↓
1.91 to 1.77 ↓
1.38 to 2.50 ↑
  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

13-cis β-carotene
(μg/g d.w.)
0.09 to 0.20 ↑
0.20 to 0.15 ↓
0.19 to 0.19 =
0.27 to 0.37 ↑
0.21 to 0.53 ↑
  • -

    100 % corn

  • -

    15% yellow peach palm

  • -

    25% yellow peach palm

  • -

    15% red peach palm

  • -

    15% red peach palm

9-cis β-carotene
(μg/g d.w.)
0.10 to 0.29 ↑
0.21 to 0.21 =
0.25 to 0.28 ↑
0.34 to 0.46 ↑
0.22 to 0.48 ↑
Corn grits with tomato powder
  • -

    single-screw polytrophic extruder, screw compression ratio of 3:1, barrel temperatures of 125–145–135 °C, die diameter of 3 mm, screw speed of 120 rpm.

  • -

    Control

  • -

    5% tomato

  • -

    10% tomato

  • -

    15% tomato

  • -

    20% tomato

  • -

    25% tomato

  • -

    30% tomato

Lycopene
(mg/100 g)
0.2 to 0.2 =
4.6 to 0.4 ↓
9.7 to 1.6 ↓
15.7 to 4.1 ↓
21.4 to 7.8 ↓
25.2 to 17.9 ↓
31.2 to 22.3 ↓
[89]

1—maize variety, = unchanged, ↑ increase, ↓ decrease.