. 2023 Jul 15;23(8):5801–5811. doi: 10.1021/acs.cgd.3c00401

Table 1. Data Extracted by the Series of 2D-GIWAXS Recorded at Different α_I for Spi SOM, Opa SOM, and CaCO₃ Mixed with Spi (Spi_mix) and with Opa (Opa_mix)^a.

	q_¹ (Å^–1)	fwhm¹ (Å^–)	q_² (Å^–1)	fwhm² (Å^–1)	A¹	A²	A²/(A² + A¹) (%)	A^s/(A^s + A^b) (%)
Spi SOM	0.38	0.08	0.68	0.16	10	33	76	from 5 (α_I l) to 40 (α_I h)
Opa SOM	0.38	0.10	0.67	0.16	9	29	76	from 5 (α_I l) to 40 (α_I h)
Spi SOM mix	0.38	0.08	0.68	0.16	4	9	70	from 0 (α_I l) to 20 (α_I h)
Opa SOM mix	0.34	0.10	0.66	0.18	2	3	60	from 0 (α_I l) to 13 (α_I h)

For the two peaks (see Figure 3) we report the position (q), the width (W), the integrated area (A) and their relative area. From the fit of the azimuthal profiles of peak 2, we determine the two Gaussian contributions [sharp (s) and broad (b), and we report their area ratio from the surface region [lowest α_I (α_I l)] to whole thickness [highest α_I (α_I h)].

Table 1. Data Extracted by the Series of 2D-GIWAXS Recorded at Different αI for Spi SOM, Opa SOM, and CaCO3 Mixed with Spi (Spi_mix) and with Opa (Opa_mix)a.

Table 1. Data Extracted by the Series of 2D-GIWAXS Recorded at Different α_I for Spi SOM, Opa SOM, and CaCO₃ Mixed with Spi (Spi_mix) and with Opa (Opa_mix)^a.