Table 3. Structure refinement statistics.
Values in parentheses are for the highest isotropic resolution shell.
Resolution (Å) | 47.53–3.13†–2.47 (2.71–2.47) |
No. of residues/non-H atoms | 266/2071 |
R work | 0.219 (0.355) |
R free | 0.255 (0.368) |
CC work | 0.993 (0.492) |
CC free | 0.913 (0.590) |
No. free reflections | 910 |
R all | 0.223 (0.379) |
Average ADP (Å2) | 82 |
R.m.s. deviations from ideal | |
Bond lengths (Å) | 0.010 |
Angles (°) | 1.755 |
Ramachandran plot | |
Allowed | 261 (99.6%) |
Outliers | 1 (0.4%) |
Solvent content (%) | 76 |
As calculated by MOLPROBITY.
The lowest high-resolution diffraction limit after the anisotropic cut-off.