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. 2023 Jan 18;15(3):344–353. doi: 10.1055/s-0042-1760668

Table 1. Optimized conditions for mass spectrometry.

Positive ion spray voltage 4,000 V
Sheath gas (Arb) 50
Auxiliary gas (Arb) 5
Sweep gas 1
Ion transfer tube temperature 200°C
Vaporizer temperature 400°C
Mobile phase A: 0.1% formic acid in water
B: Acetonitrile
Column C 18 (3.0 μm 120Å, 2.1 × 50 mm)
Flow rate 0.4 mL/min