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. 2023 Jul 31;8(32):29704–29716. doi: 10.1021/acsomega.3c03929

Table 2. Comparing TPC, TTC, Biological Activities, Recovery Yield, and Energy Consumption in Four Different Extraction Techniquesa.

criteria/extraction techniques NADES-based UMAE NADES-based MAE NADES-based UAE NADES-based MUAE
Ci-Glu
conditions        
LSR (mL/g) 40 50 40 40
water content (%) 20 20 20 20
ultrasonic power (W) 150   150 150
temperature (°C) 30   30 30
sonication time (min) 5   5 5
microwave power (W) 400 400   400
microwave irradiation time (min) 1 2   1
TPC (mg GAE/g dw) 27.07 ± 0.27a 22.13 ± 0.75c 9.56 ± 0.17d 23.88 ± 0.46b
recovery yield (%) 77.52 ± 0.78a 63.37 ± 2.15c 27.38 ± 0.49d 68.38 ± 1.32b
ABTS (μM TE/g dw) 755 ± 50a 606 ± 21b 529 ± 45c 637 ± 11b
DPPH (μM TE/g dw) 123 ± 3a 91 ± 4c 87 ± 2c 115 ± 4b
OH (mM TE/g dw) 104 ± 0.31a 100 ± 0.67b 87 ± 0.8c 104 ± 0.29a
tyrosinase inhibition (mg AE/g dw) 648 ± 29a 379 ± 33c 259 ± 43d 566 ± 43b
α-amylase inhibition (g ACE/g dw) 10.39 ± 0.06a 9.1 ± 0.37c 8.59 ± 0.1d 9.71 ± 0.08b
AChE inhibition (g TCE/g dw) 3.83 ± 0.12a 3.31 ± 0.08c 2.94 ± 0.08d 3.59 ± 0.04b
energy consumption (Wh) 19.2 13.3 12.5 19.2
Lac-Glu
conditions        
LSR (mL/g) 40 50 40 40
water content (%) 40 40 40 40
ultrasonic power (W) 600   600 600
temperature (°C) 30   30 30
sonication time (min) 5   5 5
microwave power (W) 400 400   400
microwave irradiation time (min) 1 2   1
TTC (mg UA/g dw) 111 ± 3a 90 ± 1c 69 ± 2d 104 ± 3b
recovery yield (%) 82.71 ± 2.23a 67.06 ± 0.75c 51.42 ± 1.49d 77.50 ± 2.21b
ABTS (μM TE/g dw) 900 ± 17a 722 ± 23c 663 ± 17d 842 ± 21b
DPPH (μM TE/g dw) 120 ± 1a 87 ± 1c 87 ± 3c 110 ± 3b
OH (mM TE/g dw) 52 ± 0.33a 44 ± 0.15c 36 ± 0.89d 48 ± 0.31b
tyrosinase inhibition (mg AE/g dw) 309 ± 17a 232 ± 14b 121 ± 31c 285 ± 25b
α-amylase inhibition (g ACE/g dw) 15.78 ± 0.10a 9.5 ± 0.38c 8.03 ± 0.05d 14.86 ± 0.14b
AChE inhibition (g TCE/g dw) 4.36 ± 0.09a 4.21 ± 0.11a 3.36 ± 0.07b 4.25 ± 0.04a
energy consumption (Wh) 56.67 13.3 50 56.67
a

Different characters (a, b, c, and d) showed significant statistical differences.