| Rigaku R-AXIS RAPID diffractometer | 2621 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.077 |
| ω scans | θmax = 27.5°, θmin = 2.7° |
| Absorption correction: multi-scan (ABSCOR; Rigaku, 1995) | h = −19→20 |
| Tmin = 0.815, Tmax = 0.990 | k = −7→7 |
| 15791 measured reflections | l = −26→25 |
| 3850 independent reflections |
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