Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Ni(C14H21N2S3)2] |
| M r | 685.72 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 173 |
| a, b, c (Å) | 15.5444 (6), 5.5388 (3), 20.1592 (8) |
| β (°) | 103.675 (7) |
| V (Å3) | 1686.44 (13) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.97 |
| Crystal size (mm) | 0.08 × 0.02 × 0.01 |
| Data collection | |
| Diffractometer | Rigaku R-AXIS RAPID |
| Absorption correction | Multi-scan (ABSCOR; Rigaku, 1995 ▸) |
| T min, T max | 0.815, 0.990 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 15791, 3850, 2621 |
| R int | 0.077 |
| (sin θ/λ)max (Å−1) | 0.649 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.045, 0.079, 1.00 |
| No. of reflections | 3850 |
| No. of parameters | 179 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.44, −0.27 |