S1—O6 | 1.4469 (14) | C17—H17 | 0.9500 |
S1—O4 | 1.4510 (15) | C18—C19 | 1.405 (3) |
S1—O5 | 1.4585 (15) | C18—H18 | 0.9500 |
S1—C15 | 1.7808 (18) | C19—H19 | 0.9500 |
S1—Na2i | 3.2984 (9) | C21—H21A | 0.9900 |
Na2—O5ii | 2.2500 (16) | C21—H21B | 0.9900 |
Na2—O4iii | 2.2602 (16) | C22—C23 | 1.515 (3) |
Na2—O3 | 2.4248 (15) | C22—H22A | 0.9900 |
Na2—N7 | 2.4690 (18) | C22—H22B | 0.9900 |
Na2—N11 | 2.487 (2) | C23—C24 | 1.390 (3) |
Na2—Na2iv | 3.9829 (15) | C24—C25 | 1.383 (3) |
O3—C12 | 1.354 (2) | C24—H24 | 0.9500 |
O3—H3 | 0.88 (3) | C25—C26 | 1.380 (3) |
N7—C19 | 1.312 (3) | C25—H25 | 0.9500 |
N7—C20 | 1.373 (2) | C26—C27 | 1.380 (3) |
N8—C22 | 1.449 (2) | C26—H26 | 0.9500 |
N8—C28 | 1.461 (2) | C27—H27 | 0.9500 |
N8—C21 | 1.466 (2) | C28—C29 | 1.504 (3) |
N9—C23 | 1.337 (3) | C28—H28A | 0.9900 |
N9—C27 | 1.350 (3) | C28—H28B | 0.9900 |
N10—C29 | 1.338 (3) | C29—C30 | 1.388 (3) |
N10—C33 | 1.347 (3) | C30—C31 | 1.386 (3) |
N11—C34 | 1.129 (3) | C30—H30 | 0.9500 |
C12—C13 | 1.386 (3) | C31—C32 | 1.372 (3) |
C12—C20 | 1.433 (3) | C31—H31 | 0.9500 |
C13—C14 | 1.411 (3) | C32—C33 | 1.369 (4) |
C13—C21 | 1.504 (3) | C32—H32 | 0.9500 |
C14—C15 | 1.367 (3) | C33—H33 | 0.9500 |
C14—H14 | 0.9500 | C34—C35 | 1.459 (4) |
C15—C16 | 1.427 (3) | C35—H35A | 0.9800 |
C16—C20 | 1.413 (3) | C35—H35B | 0.9800 |
C16—C17 | 1.423 (3) | C35—H35C | 0.9800 |
C17—C18 | 1.356 (3) | ||
O6—S1—O4 | 113.25 (9) | C17—C18—H18 | 120.3 |
O6—S1—O5 | 113.25 (9) | C19—C18—H18 | 120.3 |
O4—S1—O5 | 112.87 (9) | N7—C19—C18 | 123.96 (19) |
O6—S1—C15 | 106.16 (9) | N7—C19—H19 | 118.0 |
O4—S1—C15 | 105.55 (9) | C18—C19—H19 | 118.0 |
O5—S1—C15 | 104.82 (9) | N7—C20—C16 | 122.71 (17) |
O6—S1—Na2i | 139.46 (6) | N7—C20—C12 | 117.21 (16) |
O4—S1—Na2i | 34.63 (6) | C16—C20—C12 | 120.07 (16) |
O5—S1—Na2i | 79.43 (7) | N8—C21—C13 | 110.84 (15) |
C15—S1—Na2i | 107.18 (6) | N8—C21—H21A | 109.5 |
O5ii—Na2—O4iii | 127.68 (7) | C13—C21—H21A | 109.5 |
O5ii—Na2—O3 | 101.42 (6) | N8—C21—H21B | 109.5 |
O4iii—Na2—O3 | 92.56 (6) | C13—C21—H21B | 109.5 |
O5ii—Na2—N7 | 130.30 (7) | H21A—C21—H21B | 108.1 |
O4iii—Na2—N7 | 101.50 (6) | N8—C22—C23 | 113.07 (16) |
O3—Na2—N7 | 65.83 (5) | N8—C22—H22A | 109.0 |
O5ii—Na2—N11 | 88.66 (7) | C23—C22—H22A | 109.0 |
O4iii—Na2—N11 | 104.46 (7) | N8—C22—H22B | 109.0 |
O3—Na2—N11 | 148.91 (7) | C23—C22—H22B | 109.0 |
N7—Na2—N11 | 85.14 (7) | H22A—C22—H22B | 107.8 |
O5ii—Na2—S1iii | 113.91 (5) | N9—C23—C24 | 122.47 (19) |
O4iii—Na2—S1iii | 21.39 (4) | N9—C23—C22 | 118.05 (17) |
O3—Na2—S1iii | 112.83 (4) | C24—C23—C22 | 119.46 (19) |
N7—Na2—S1iii | 115.19 (5) | C25—C24—C23 | 118.7 (2) |
N11—Na2—S1iii | 88.83 (6) | C25—C24—H24 | 120.6 |
O5ii—Na2—Na2iv | 57.30 (5) | C23—C24—H24 | 120.6 |
O4iii—Na2—Na2iv | 76.32 (5) | C26—C25—C24 | 119.3 (2) |
O3—Na2—Na2iv | 132.85 (5) | C26—C25—H25 | 120.3 |
N7—Na2—Na2iv | 160.89 (5) | C24—C25—H25 | 120.3 |
N11—Na2—Na2iv | 77.20 (6) | C25—C26—C27 | 118.6 (2) |
S1iii—Na2—Na2iv | 57.86 (2) | C25—C26—H26 | 120.7 |
C12—O3—Na2 | 120.18 (11) | C27—C26—H26 | 120.7 |
C12—O3—H3 | 114.9 (16) | N9—C27—C26 | 122.8 (2) |
Na2—O3—H3 | 120.7 (16) | N9—C27—H27 | 118.6 |
S1—O4—Na2i | 123.98 (9) | C26—C27—H27 | 118.6 |
S1—O5—Na2v | 148.14 (10) | N8—C28—C29 | 112.78 (16) |
C19—N7—C20 | 117.48 (17) | N8—C28—H28A | 109.0 |
C19—N7—Na2 | 124.08 (13) | C29—C28—H28A | 109.0 |
C20—N7—Na2 | 117.42 (12) | N8—C28—H28B | 109.0 |
C22—N8—C28 | 111.39 (16) | C29—C28—H28B | 109.0 |
C22—N8—C21 | 112.06 (15) | H28A—C28—H28B | 107.8 |
C28—N8—C21 | 111.93 (15) | N10—C29—C30 | 122.79 (19) |
C23—N9—C27 | 118.06 (18) | N10—C29—C28 | 115.47 (18) |
C29—N10—C33 | 116.2 (2) | C30—C29—C28 | 121.73 (18) |
C34—N11—Na2 | 151.4 (2) | C31—C30—C29 | 119.4 (2) |
O3—C12—C13 | 124.01 (17) | C31—C30—H30 | 120.3 |
O3—C12—C20 | 116.23 (16) | C29—C30—H30 | 120.3 |
C13—C12—C20 | 119.75 (17) | C32—C31—C30 | 118.4 (2) |
C12—C13—C14 | 119.07 (17) | C32—C31—H31 | 120.8 |
C12—C13—C21 | 120.28 (17) | C30—C31—H31 | 120.8 |
C14—C13—C21 | 120.64 (16) | C33—C32—C31 | 118.5 (2) |
C15—C14—C13 | 122.77 (17) | C33—C32—H32 | 120.8 |
C15—C14—H14 | 118.6 | C31—C32—H32 | 120.8 |
C13—C14—H14 | 118.6 | N10—C33—C32 | 124.7 (2) |
C14—C15—C16 | 119.26 (17) | N10—C33—H33 | 117.6 |
C14—C15—S1 | 119.96 (14) | C32—C33—H33 | 117.6 |
C16—C15—S1 | 120.78 (14) | N11—C34—C35 | 179.4 (3) |
C20—C16—C17 | 117.06 (17) | C34—C35—H35A | 109.5 |
C20—C16—C15 | 119.07 (17) | C34—C35—H35B | 109.5 |
C17—C16—C15 | 123.87 (17) | H35A—C35—H35B | 109.5 |
C18—C17—C16 | 119.36 (19) | C34—C35—H35C | 109.5 |
C18—C17—H17 | 120.3 | H35A—C35—H35C | 109.5 |
C16—C17—H17 | 120.3 | H35B—C35—H35C | 109.5 |
C17—C18—C19 | 119.39 (19) | ||
O6—S1—O4—Na2i | −146.44 (9) | Na2—N7—C20—C12 | −13.3 (2) |
O5—S1—O4—Na2i | −16.08 (13) | C17—C16—C20—N7 | −0.6 (3) |
C15—S1—O4—Na2i | 97.84 (10) | C15—C16—C20—N7 | 179.29 (17) |
O6—S1—O5—Na2v | 78.3 (2) | C17—C16—C20—C12 | −179.41 (17) |
O4—S1—O5—Na2v | −52.0 (2) | C15—C16—C20—C12 | 0.5 (3) |
C15—S1—O5—Na2v | −166.41 (18) | O3—C12—C20—N7 | −0.3 (2) |
Na2i—S1—O5—Na2v | −61.26 (19) | C13—C12—C20—N7 | −178.66 (16) |
Na2—O3—C12—C13 | −167.32 (14) | O3—C12—C20—C16 | 178.61 (16) |
Na2—O3—C12—C20 | 14.4 (2) | C13—C12—C20—C16 | 0.2 (3) |
O3—C12—C13—C14 | −179.49 (17) | C22—N8—C21—C13 | −163.21 (16) |
C20—C12—C13—C14 | −1.2 (3) | C28—N8—C21—C13 | 70.82 (19) |
O3—C12—C13—C21 | 1.3 (3) | C12—C13—C21—N8 | 63.1 (2) |
C20—C12—C13—C21 | 179.60 (16) | C14—C13—C21—N8 | −116.12 (18) |
C12—C13—C14—C15 | 1.6 (3) | C28—N8—C22—C23 | −155.23 (16) |
C21—C13—C14—C15 | −179.20 (17) | C21—N8—C22—C23 | 78.5 (2) |
C13—C14—C15—C16 | −0.9 (3) | C27—N9—C23—C24 | −1.4 (3) |
C13—C14—C15—S1 | 179.41 (14) | C27—N9—C23—C22 | 176.90 (19) |
O6—S1—C15—C14 | −126.08 (15) | N8—C22—C23—N9 | 6.4 (3) |
O4—S1—C15—C14 | −5.59 (17) | N8—C22—C23—C24 | −175.17 (18) |
O5—S1—C15—C14 | 113.80 (16) | N9—C23—C24—C25 | 1.3 (3) |
Na2i—S1—C15—C14 | 30.51 (16) | C22—C23—C24—C25 | −177.0 (2) |
O6—S1—C15—C16 | 54.26 (17) | C23—C24—C25—C26 | 0.1 (3) |
O4—S1—C15—C16 | 174.74 (15) | C24—C25—C26—C27 | −1.3 (3) |
O5—S1—C15—C16 | −65.86 (17) | C23—N9—C27—C26 | 0.2 (3) |
Na2i—S1—C15—C16 | −149.16 (13) | C25—C26—C27—N9 | 1.2 (4) |
C14—C15—C16—C20 | −0.1 (3) | C22—N8—C28—C29 | 72.0 (2) |
S1—C15—C16—C20 | 179.53 (13) | C21—N8—C28—C29 | −161.71 (16) |
C14—C15—C16—C17 | 179.75 (18) | C33—N10—C29—C30 | 0.6 (3) |
S1—C15—C16—C17 | −0.6 (3) | C33—N10—C29—C28 | −178.2 (2) |
C20—C16—C17—C18 | 1.6 (3) | N8—C28—C29—N10 | −145.01 (18) |
C15—C16—C17—C18 | −178.31 (19) | N8—C28—C29—C30 | 36.2 (3) |
C16—C17—C18—C19 | −0.9 (3) | N10—C29—C30—C31 | −0.4 (3) |
C20—N7—C19—C18 | 1.9 (3) | C28—C29—C30—C31 | 178.36 (19) |
Na2—N7—C19—C18 | −166.24 (17) | C29—C30—C31—C32 | −0.3 (3) |
C17—C18—C19—N7 | −0.9 (4) | C30—C31—C32—C33 | 0.7 (3) |
C19—N7—C20—C16 | −1.1 (3) | C29—N10—C33—C32 | −0.2 (4) |
Na2—N7—C20—C16 | 167.84 (13) | C31—C32—C33—N10 | −0.4 (4) |
C19—N7—C20—C12 | 177.74 (18) |