| Rigaku R-AXIS RAPID diffractometer | 4023 reflections with F2 > 2.0σ(F2) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.042 |
| ω scans | θmax = 27.4°, θmin = 2.5° |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −13→13 |
| Tmin = 0.867, Tmax = 0.971 | k = −18→18 |
| 23162 measured reflections | l = −20→21 |
| 5490 independent reflections |
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