| Bruker Kappa APEXII area-detector diffractometer | 5446 reflections with I > 2σ(I) |
| ω– and φ–scans | Rint = 0.021 |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | θmax = 35.2°, θmin = 4.3° |
| Tmin = 0.515, Tmax = 0.669 | h = −11→11 |
| 30601 measured reflections | k = −12→12 |
| 6766 independent reflections | l = −22→21 |