| Bruker Kappa APEXII area-detector diffractometer | 1745 reflections with I > 2σ(I) |
| ω– and φ–scans | Rint = 0.014 |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | θmax = 35.2°, θmin = 4.4° |
| Tmin = 0.630, Tmax = 0.719 | h = −16→16 |
| 13071 measured reflections | k = −10→10 |
| 1745 independent reflections | l = −17→16 |