Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C38H28O6 |
| M r | 580.60 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 302 |
| a, b, c (Å) | 9.5219 (2), 10.1010 (2), 30.7050 (8) |
| β (°) | 96.666 (1) |
| V (Å3) | 2933.26 (11) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 0.72 |
| Crystal size (mm) | 0.32 × 0.28 × 0.21 |
| Data collection | |
| Diffractometer | Bruker SMART APEXII CCD |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 14741, 4775, 4298 |
| R int | 0.032 |
| (sin θ/λ)max (Å−1) | 0.585 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.042, 0.142, 1.06 |
| No. of reflections | 4775 |
| No. of parameters | 397 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.24, −0.23 |