Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Ni(C12H14O4)(C16H18N4)] |
| M r | 547.28 |
| Crystal system, space group | Monoclinic, C2/m |
| Temperature (K) | 293 |
| a, b, c (Å) | 14.489 (3), 20.198 (4), 10.741 (2) |
| β (°) | 127.46 (3) |
| V (Å3) | 2495.2 (12) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.82 |
| Crystal size (mm) | 0.60 × 0.20 × 0.10 |
| Data collection | |
| Diffractometer | Rigaku Mercury CCD |
| Absorption correction | Multi-scan (Jacobson, 1998 ▸) |
| T min, T max | 0.639, 0.922 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 12149, 2343, 1975 |
| R int | 0.060 |
| (sin θ/λ)max (Å−1) | 0.602 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.065, 0.148, 1.15 |
| No. of reflections | 2343 |
| No. of parameters | 174 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.39, −0.42 |