| Crystal data |
| Chemical formula |
C16H22O2
|
|
M
r
|
246.33 |
| Crystal system, space group |
Monoclinic, P2/c
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
10.4134 (2), 6.9167 (2), 20.4801 (5) |
| β (°) |
90.308 (2) |
|
V (Å3) |
1475.09 (6) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.56 |
| Crystal size (mm) |
0.30 × 0.24 × 0.15 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Single source at home/near, HyPix3000 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2020 ▸) |
|
T
min, T
max
|
0.960, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
13939, 2866, 2161 |
|
R
int
|
0.038 |
| (sin θ/λ)max (Å−1) |
0.615 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.044, 0.129, 1.07 |
| No. of reflections |
2866 |
| No. of parameters |
166 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.12, −0.16 |
