Table 1.
Data collection and refinement statistics
| Dataset | Native |
|---|---|
| Data collection | |
| Beamline | SSRL 9–2 |
| Space group | P65 |
| Cell dimensions | |
| a, b, c (Å) | 123.3, 123.3, 136.9 |
| α, β, γ (deg) | 90.0, 90.0, 120 |
| Wavelength (Å) | 0.88684 |
| Resolution† (Å) | 50–2.95 (3.06–2.95)* |
| R merge(%) | 18.8 (135.6) |
| CC1/2 | 0.994 (0.766) |
| I / σI | 20.0 (2.0) |
| Observations | 49009 (4849) |
| Unique reflections | 24916 (2453) |
| Multiplicity | 20.5 (16) |
| Completeness (%) | 100.0 (99.8) |
| Resolution (Å) | 50–2.95 (3.06–2.95) |
| No. reflections | 24916 |
| Refinement R work/Rfree (%) | 18.5/21.5 |
| No. atoms | |
| Protein | 4578 |
| Water | 0 |
| Ligands | 0 |
| B-factors | |
| mean | 76.2 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.002 |
| Bond angles (deg) | 0.52 |
| Ramachandran | |
| Favored (%) | 96.33 |
| Allowed (%) | 3.77 |
| Outliers (%) | 0 |
| Clashscore | 3.4 |
*Values in parentheses are for highest-resolution shell.
†Resolution limit used the criterion of I/σI > 2.0