Table 2.
Overview of the methodological characteristics including Linearity range, correlation coefficient (R2), limits of detection (LOD); limits of quantification (LOQ) and recovery for the analysis of mycotoxins in beers.
| Mycotoxins | Linearity Range (µg/L) |
Correlation Coefficient (R2) |
LOD (µg/L) |
LOQ (µg/L) |
Recovery ± RSD (%, n = 6) | ||
|---|---|---|---|---|---|---|---|
| Spiked Low | Spiked Middle | Spiked High | |||||
| DON | 15–250 | 0.9996 | 5 | 15 | 121.9 (10.0) |
91.1 (3.1) |
94.4 (4.2) |
| D3G | 15–100 | 0.9965 | 5 | 15 | 109.1 (13.5) |
104.8 (12.2) |
82.1 (7.1) |
| 3A-DON | 30–500 | 0.9911 | 10 | 30 | 119.2 (11.1) |
103.3 (2.3) |
106.0 (1.0) |
| 15A-DON | 30–500 | 0.9873 | 10 | 30 | 115.8 (10.6) |
102.2 (2.8) |
89.8 (1.8) |
| NIV | 150–2500 | 0.9990 | 50 | 150 | 80.7 (10.6) |
104.0 (3.4) |
88.9 (3.8) |
| ZEN | 15–250 | 0.9941 | 5 | 15 | 111.6 (5.7) |
112.6 (2.8) |
80.6 (3.2) |
| FB1 | 15–250 | 0.9947 | 5 | 15 | 110.4 (15.7) |
86.7 (9.7) |
80.2 (5.4) |
| OTA | 1.5–25 | 0.9998 | 0.5 | 1.5 | 121.6 (3.2) |
92.0 (2.4) |
88.1 (1.4) |