Table 9. Selected Distances and Angles for 7 and 12·0.4CHCl₃ (in Å and deg)^a.

Parameter	7 (X = void)	12·0.4CHCl3 (X = Cl)b
Au–Cl	2.2922(7)	2.2864(7)
Au–P	2.2268(7)	2.2286(6)
P–Au–Cl	174.47(3)	175.34(3)
Sb–X1/2	na	2.4356(6)/2.4875(6)
Sb–C1	2.130(2)	2.096(2)
Sb–C23/C29	2.157(3)/2.152(2)	2.107(2)/2.121(3)
C1–Sb–C23/C29	95.03(9)/95.16(9)	117.08(8)/128.10(9)
C23–Sb–C29	95.95(9)	114.71(9)
P–C6	1.787(2)	1.786(2)
P–C11/C17	1.841(2)/1.818(3)	1.811(2)/1.819(2)
C6–P–C11/17	106.2(1)/103.9(1)	108.1(1)/103.7(1)
C11–P–C17	105.4(1)	103.7(1)
Fe–C	2.028(3)–2.064(3)	2.034(2)–2.062(2)
tilt	2.1(2)	1.1(2)
τ	160.8(2)	174.0(2)

^aParameters are defined as for the other compounds discussed in this paper; see the footnote to Table 3. na = not applicable.

^bFurther data: Cl–Sb–Cl = 179.49(2)°, Cl–Sb–C (range) = 88.57(6)–91.38(6)°.