Parameter (unit) | Batch Number | Analytical method | |||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Barley to rice ratio | 70:30 | 60:40 | 45:55 | ||||||||||||
#5 | #7 | #19 | #24 | #25 | #29 | #37 | #30 | #31 | #10 | #11 | #12 | #13 | #14 | ||
Phytic acid (%) | < 0.14 | / | < 0.14 | < 0.14 | < 0.14 | < 0.14 | / | < 0.14 | < 0.14 | < 0.14 | < 0.14 | < 0.14 | < 0.14 | < 0.14 | Analytical Biochemistry Vol. 77:536–539 (1977) |
Sum of ergot alkaloids (μg/kg) | < 3.0 (LOQ) | / | < 3.0 | / | / | < 3.0 | 6.2 | 6.8 | 30.0 | / | < 3.0 | 49.1 | 50.1 | 109.5 | Internal Method, LC–MS/MS |
Patulin (μg/kg) | < 20 | / | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | < 20 | Internal Method, LC–MS/MS |
Trypsin inhibitor (TIU/g) | 1500 | 2300 | 1800 | 461 | 503 | 3300 | / | / | / | 1600 | 1600 | 1600 | < 1200 | < 1000 | AOCS Ba 12–75 |
Lectin (mg/g) | < 0.05 | < 0.05 | < 0.05 | < 0.05 | < 0.05 | < 0.05 | / | / | / | < 0.05 | < 0.05 | < 0.05 | < 0.05 | < 0.05 | J Food Sci Biotech Vol 15 No. 1 pp. 95–95 2006 mod |
AOCS: American Oil Chemists' Society; LC–MS/MS: liquid chromatography–tandem mass spectrometry; LOQ: limit of quantification; /: not provided.