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. 2023 Aug 17;88(17):12821–12825. doi: 10.1021/acs.joc.3c01089

Table 2. Pyrrole Reaction Optimizationa.

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entry deviation yield of 2ab
1 none 70%
2 DMF (0.1 M) 55%
3 50 °Cc 56%
4 NHC 1c 24%
a

0.1 mmol scale.

b

Isolated yield.

c

16 h reaction time at 50 °C.