Skip to main content
. 2023 Aug 23;62(35):14318–14325. doi: 10.1021/acs.inorgchem.3c01725

Table 1. Selected Crystallographic Parameters of (C4H12N2)2[UO2Cl4(H2O)]Cl2(s).

empirical formula (C4H12N2)2[UO2Cl4(H2O)]Cl2 μ(mm–1) 8.731
crystal color and habit yellow prismatic F(000) 1276.0
formula weight 676.04 Θ range (°) 4.504–50.692
crystal system orthorhombic limiting indices –14 ≤ h ≤ 14
a (Å) 12.2130(7)   –14 ≤ k ≤ 14
b (Å) 12.4456(7)   –16 ≤ l ≤ 16
c (Å) 13.4579(8) ref collected/unique 100 055
α (°) 90° Rint 0.0621
β (°) 90° data/restraints/parameters 1953/0/114
γ (°) 90° GOF on F2 1.198
volume (Å3) 2045.6(2) final R indices ([I > 2σ(I)]) R1 0.0113
temperature (K) 102.07 final R indices ([I > 2σ(I)]) wR2 0.0266
density, ρ (g cm–3) 2.195 R indices (all data) R1 0.0116
space group Pnma R indices (all data) wR2 0.0267
Z 4 largest diff. peak/hole (e Å–3) 0.51 and −0.98
radiation type Mo Kα (λ = 0.71073) CCDC deposition number 2 241 014