Table 2. Experimental details.

Crystal data
Chemical formula	C6H4O3S2
M r	188.23
Crystal system, space group	Triclinic, P
Temperature (K)	295
a, b, c (Å)	5.398 (1), 7.5537 (15), 9.2566 (18)
α, β, γ (°)	89.273 (6), 87.361 (6), 75.701 (5)
V (Å3)	365.36 (12)
Z	2
Radiation type	Mo Kα
μ (mm−1)	0.68
Crystal size (mm)	0.42 × 0.38 × 0.17
Data collection
Diffractometer	Bruker D8 Quest Eco
Absorption correction	Multi-scan (SADABS; Bruker, 2016 ▸)
T min, T max	0.648, 0.746
No. of measured, independent and observed [I ≥ 2u(I)] reflections	16978, 1669, 1338
R int	0.046
(sin θ/λ)max (Å−1)	0.651
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.033, 0.074, 1.11
No. of reflections	1669
No. of parameters	136
H-atom treatment	All H-atom parameters refined
Δρmax, Δρmin (e Å−3)	0.45, −0.25

Computer programs: APEX3 and SAINT (Bruker, 2018 ▸), SHELXT2014 (Sheldrick, 2015a ▸), SHELXL2016 (Sheldrick, 2015b ▸), olex2.refine (Bourhis et al., 2015 ▸), OLEX2 (Dolomanov et al., 2009 ▸), Mercury (Macrae et al., 2020 ▸), WebMO (Schmidt & Polik, 2016 ▸), and publCIF (Westrip, 2010 ▸).