| Crystal data |
| Chemical formula |
[Cu2(C9H6O4)2(C16H20N4)] |
|
M
r
|
751.71 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
173 |
|
a, b, c (Å) |
8.5431 (8), 9.7391 (9), 9.9667 (9) |
| α, β, γ (°) |
104.523 (1), 93.049 (1), 99.966 (1) |
|
V (Å3) |
786.57 (13) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.41 |
| Crystal size (mm) |
0.20 × 0.11 × 0.07 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2014 ▸) |
|
T
min, T
max
|
0.693, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
10964, 2883, 2459 |
|
R
int
|
0.042 |
| (sin θ/λ)max (Å−1) |
0.602 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.044, 0.114, 1.12 |
| No. of reflections |
2883 |
| No. of parameters |
217 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.53, −0.32 |
