| Rigaku Xcalibur Eos diffractometer | 2644 independent reflections |
| Radiation source: fine-focus sealed X-ray tube, Enhance (Mo) X-ray Source | 2204 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.044 |
| Detector resolution: 16.1593 pixels mm-1 | θmax = 28.3°, θmin = 2.4° |
| ω scans | h = −19→19 |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2022) | k = −23→23 |
| Tmin = 0.573, Tmax = 1.000 | l = −10→10 |
| 16993 measured reflections |
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