Table 1. An excerpt from the dataset presents five examples of input and output pairs.
| Original sentence | Structured format |
|---|---|
| To a solution of 3-cyano-4-((1-methylethyl)oxy)benzoic acid (200 mg) in tetrahydrofuran (THF) (10 mL) was added EDC (374 mg) and HOBt (299 mg). | MAKESOLUTION with 3-cyano-4-((1-methylethyl)oxy)benzoic acid (200 mg) and tetrahydrofuran (THF) (10 mL); ADD SLN; ADD EDC (374 mg); ADD HOBt (299 mg). |
| The resulting orange solution was partitioned between dichloromethane (10 mL) and water (10 mL) | PARTITION with dichloromethane (10 mL) and water (10 mL). |
| Ethanol and water are added to produce a solid which is collected by filtration. | ADD Ethanol; ADD water; FILTER keep precipitate. |
| The solution was quenched with saturated aqueous NH4Cl and extracted with CH2Cl2. | QUENCH with saturated aqueous NH4Cl; EXTRACT with CH2Cl2. |
| The resulting mixture was filtered and the filtrate was concentrated and the residue was purified by flash column chromatography (ethylacetate/petroleum ether gradient) to afford 1-benzyl-2-(chloromethyl)pyrrolidine. | FILTER keep filtrate; CONCENTRATE; PURIFY: ethyl acetate:petroleum ether; YIELD 1-benzyl-2-(chloromethyl)pyrrolidine. |