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. 2023 Aug 24;5(9):7652–7657. doi: 10.1021/acsapm.3c01628

Table 2. Initially Tried Recipes for Polymerization Were Tried under a Coverslip.

        Thickness (nm)
# [M]b (mM) [Cu]c (mM) [RA]d (mM) 2 h 4 h
1 620 0.063 3.1 141 98a
2 620 0.063 1.5 115 123
3 620 0.063 10.0 62 76
4 1000 0.200 2.0 220 37a
a

These samples were inhomogeneous and therefore measured thinner by ellipsometry.

b

Monomer (SPMA) concentration.

c

Copper catalyst concentration.

d

Reducing agent (ascorbic acid) concentration.