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Previous and new work on the preparation of low-valent titanium diamido compounds. (a) Reduction of a tripyrrole Ti(IV) species. (b) Incorporation of the diamido-diimine, dadi, ligand to a Ti(II) precursor. (c) Installation of a 2,6-bis(pyrrolyl)pyridine ligand to the Ti(III) precursor [TiCl3(thf)3].
