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. 2023 Sep 4;5(19):5165–5213. doi: 10.1039/d3na00163f

Nanoflowers are synthesized by a solvothermal process under diverse reaction conditions.

Nanostructure/morphology Size Reaction conditions Time and temperature in the autoclave Surfactant or template Ref.
TiO2 nanoflowers 47.56–274.36 nm NaOH (0.024 M) + 8 mL TiCl3 + 60 mL ethanol 18 h, 130 °C 34
Porous NiO nanoflowers 0.5 g Ni(ac)2·4H2O + 0.25 g urea + 30 mL ethanol 3–24 h, 190 °C 100
Zn-doped CuS nanoflowers 1 μm 0.25 mmol CuCl + 0.25 mmol Zn(Ac)2·2H2O + 0.75 mmol S powder + 15 mL ethanol 24 h, 180 °C 101
Mo-doped Bi2Se3 nanoflowers 100–200 nm 0.85 mmol Bi(NO3)3·5H2O + 0.15 mmol (NH4)6Mo7O24·4H2O+ 18 mL N,N-dimethylformamide + ammonia + Se powder + Na2SO3 20 h, 160 °C 102
Bi2O2.33 nanoflowers 0.11 g NaBiO3 + 20 mL ethanol, + 5.0 mL distilled water + 2.0 mL 1 M HNO3 solution 3–5 h, 100 °C PVP 103