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. 2023 Sep 8;12(9):1742. doi: 10.3390/antiox12091742

Table 1.

Phenolic compounds determined in mandarin peel, control, and fortified wheat bread extracts. Data are expressed as mean ± standard deviation (n = 3).

Compound (µg·g−1 DW) Mandarin Peel Control
Bread
2% (w/v)
Fortified Bread
4% (w/v)
Fortified Bread
Gallic acid 280 ± 6 a 3.52 ± 0.01 c 5.3 ± 0.5 b 5.6 ± 0.5 b
Dihydroxybenzoic acid n.d. 0.29 ± 0.02 b 0.42 ± 0.03 a 0.44 ± 0.02 a
Caffeic acid 38 ± 1 a n.d. n.d. 0.75 ± 0.02 b
p-Coumaric acid 72.4 ± 0.2 a 3.50 ± 0.07 b 2.28 ± 0.07 c 2.34 ± 0.09 c
trans-Ferulic acid 96.2 ± 0.5 a 2.01 ± 0.03 c 2.4 ± 0.2 bc 2.57 ± 0.08 b
Rutin 45 ± 4 a 2.06 ± 0.01 c n.a. 7.3 ± 0.5 b
Naringin 13 ± 1 a n.d. n.a. 3.0 ± 0.2 b
Hesperidin (6.2 ± 0.9) × 103 a 1.1 ± 0.4 c n.a. 83 ± 3 b
Myricetin 138 ± 20 a n.d. n.a. 16.6 ± 0.9 b
Resveratrol n.d. 0.502 ± 0.001 a 0.501 ± 0.001 a 0.502 ± 0.002 a
Quercetin 63 ± 3 a n.d. 22.8 ± 0.6 c 33.3 ± 0.6 b
Kaempferol 56 ± 8 n.d. n.d. n.d.
Total Phenolic Acids 489 ± 8 a 9.3 ± 0.1 b 10.7 ± 0.03 b 12.4 ± 0.3 b
Total Flavonoids 6400 ± 900 a/
119 ± 10 a
3.1 ± 0.4 d/
0.502 ± 0.01 c
22.7 ± 0.2 c 141 ± 3 b/
33.8 ± 0.2 b
Total Polyphenols 6900 ± 940 a/
607 ± 18 a
12.9 ± 0.3 d/
9.8 ± 0.1 c
33.8 ± 0.2 c 154 ± 3 b/
46.3 ± 0.9 b

Mean values with different letters in the same column indicate significant differences (p-value < 0.05) according to ANOVA and Fisher LSD test. n.d. = not detected; n.a. = not analyzed. Total values in italics exclude hesperidin, myricetin, rutin, and naringin. DW: dry weight (moisture content of: mandarin peels (38.8 ± 0.6)%, control bread (33.8 ± 0.3)%, 2% (w/v) enriched bread (29.4 ± 0.5)%, and 4% (w/v) enriched bread (28.8 ± 0.4)%).