Skip to main content
. 2023 Sep 20;8(39):36401–36411. doi: 10.1021/acsomega.3c05293

Table 1. Optimization with the BDMS Catalyst.

entry BDMS (mol %) solvent time (minutes) yield (%)
1 5   5 55
2 10   5 70
3 10   10 95
4 15   20 85
5 20   60 90
6 10 CH3OH 120 50
7 10 CH2Cl2 120 40
8 10 CHCl3 60 60
9 10 C2H5CO2CH3 120 70
10 10 CH3CN 60 50