| Xcalibur, Eos diffractometer | 5510 independent reflections |
| Radiation source: fine-focus sealed X-ray tube, Enhance (Mo) X-ray Source | 2962 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.092 |
| Detector resolution: 16.1593 pixels mm-1 | θmax = 29.3°, θmin = 2.0° |
| ω scans | h = −17→14 |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2022) | k = −11→13 |
| Tmin = 0.995, Tmax = 1.000 | l = −30→45 |
| 18857 measured reflections |
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