| Crystal data |
| Chemical formula |
[CoCl2(C4H4N2)] |
|
M
r
|
209.92 |
| Crystal system, space group |
Orthorhombic, I
m
m
a
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
6.6935 (1), 7.2024 (1), 12.7978 (2) |
|
V (Å3) |
616.97 (2) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
28.91 |
| Crystal size (mm) |
0.1 × 0.08 × 0.08 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy, Dualflex, HyPix |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2022 ▸) |
|
T
min, T
max
|
0.316, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
3164, 395, 386 |
|
R
int
|
0.027 |
| (sin θ/λ)max (Å−1) |
0.639 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.020, 0.058, 1.07 |
| No. of reflections |
395 |
| No. of parameters |
30 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.64, −0.34 |
