Synthesis and crystal structure of bis­(tert-butyl isocyanide-κC)[5,10,15,20-tetra­kis­(4-chloro­phen­yl)porphyrinato-κ4 N]iron(II)

. 2023 Sep 26;79(Pt 10):931–935. doi: 10.1107/S2056989023008083

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Fe	0.00822 (17)	0.01188 (16)	0.01215 (17)	−0.00047 (13)	0.00312 (13)	0.00022 (13)
C23	0.0088 (8)	0.0138 (8)	0.0178 (9)	−0.0010 (6)	0.0024 (7)	−0.0018 (7)
N3	0.0138 (7)	0.0197 (8)	0.0167 (8)	0.0018 (6)	0.0053 (6)	−0.0003 (6)
C24	0.0179 (9)	0.0241 (9)	0.0198 (9)	0.0024 (8)	0.0102 (8)	0.0065 (8)
C25	0.0253 (11)	0.0195 (9)	0.0401 (12)	0.0018 (8)	0.0154 (10)	0.0045 (9)
C26	0.0185 (11)	0.0500 (14)	0.0349 (12)	−0.0002 (10)	0.0095 (9)	0.0147 (11)
C27	0.0425 (13)	0.0337 (12)	0.0243 (11)	0.0067 (10)	0.0207 (10)	0.0053 (9)
N1	0.0107 (7)	0.0130 (7)	0.0132 (7)	−0.0004 (5)	0.0049 (6)	0.0000 (6)
N2	0.0084 (7)	0.0133 (7)	0.0138 (7)	−0.0003 (5)	0.0031 (6)	0.0001 (6)
C1	0.0104 (8)	0.0171 (8)	0.0136 (8)	0.0003 (7)	0.0049 (7)	−0.0003 (7)
C2	0.0101 (8)	0.0192 (9)	0.0175 (9)	0.0013 (7)	0.0032 (7)	0.0019 (7)
C3	0.0145 (9)	0.0178 (9)	0.0194 (9)	0.0024 (7)	0.0060 (7)	0.0025 (7)
C4	0.0123 (8)	0.0155 (8)	0.0132 (8)	0.0025 (7)	0.0051 (7)	0.0016 (7)
C5	0.0151 (9)	0.0137 (8)	0.0132 (8)	0.0009 (7)	0.0062 (7)	0.0000 (7)
C6	0.0149 (9)	0.0128 (8)	0.0136 (8)	−0.0002 (7)	0.0056 (7)	−0.0009 (7)
C7	0.0163 (9)	0.0136 (8)	0.0214 (9)	−0.0022 (7)	0.0060 (8)	−0.0002 (7)
C8	0.0135 (9)	0.0160 (9)	0.0220 (9)	−0.0043 (7)	0.0054 (8)	−0.0023 (7)
C9	0.0124 (8)	0.0171 (8)	0.0128 (8)	−0.0026 (7)	0.0047 (7)	−0.0017 (7)
C10	0.0105 (8)	0.0177 (8)	0.0118 (8)	−0.0012 (7)	0.0036 (7)	−0.0012 (7)
C11	0.0131 (9)	0.0149 (8)	0.0187 (9)	−0.0001 (7)	0.0078 (7)	0.0002 (7)
C12	0.0162 (9)	0.0167 (8)	0.0181 (9)	−0.0008 (7)	0.0062 (7)	−0.0008 (7)
C13	0.0147 (9)	0.0205 (9)	0.0212 (9)	0.0029 (7)	0.0072 (8)	0.0049 (7)
C14	0.0157 (9)	0.0119 (8)	0.0309 (11)	0.0018 (7)	0.0112 (8)	−0.0006 (7)
C15	0.0194 (10)	0.0205 (9)	0.0226 (10)	0.0020 (8)	0.0061 (8)	−0.0055 (8)
C16	0.0191 (9)	0.0205 (9)	0.0176 (9)	0.0029 (7)	0.0058 (8)	−0.0004 (7)
C17	0.0103 (8)	0.0114 (8)	0.0202 (9)	0.0009 (6)	0.0035 (7)	0.0007 (7)
C18	0.0137 (9)	0.0317 (11)	0.0204 (10)	−0.0021 (8)	0.0071 (8)	−0.0027 (8)
C19	0.0150 (9)	0.0300 (10)	0.0215 (10)	−0.0030 (8)	0.0029 (8)	−0.0071 (8)
C20	0.0088 (8)	0.0187 (9)	0.0312 (10)	−0.0037 (7)	0.0041 (8)	0.0001 (8)
C21	0.0173 (10)	0.0489 (13)	0.0257 (11)	−0.0065 (9)	0.0109 (9)	0.0028 (10)
C22	0.0163 (10)	0.0453 (13)	0.0185 (10)	−0.0059 (9)	0.0061 (8)	−0.0032 (9)
Cl2	0.0135 (2)	0.0395 (3)	0.0448 (3)	−0.0117 (2)	0.0056 (2)	−0.0006 (2)
Cl1	0.0304 (3)	0.0139 (2)	0.0455 (3)	0.00429 (19)	0.0091 (2)	0.0003 (2)