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. 2023 Sep 26;79(Pt 10):931–935. doi: 10.1107/S2056989023008083
Fe—C23 1.9244 (18) C5—C11 1.496 (2)
Fe—C23i 1.9244 (18) C6—C7 1.443 (2)
Fe—N1i 2.0074 (14) C7—C8 1.350 (3)
Fe—N1 2.0074 (14) C7—H7 0.9500
Fe—N2i 2.0081 (14) C8—C9 1.434 (2)
Fe—N2 2.0081 (14) C8—H8 0.9500
C23—N3 1.159 (2) C9—C10i 1.398 (2)
N3—C24 1.464 (2) C10—C9i 1.398 (2)
C24—C26 1.520 (3) C10—C17 1.506 (2)
C24—C25 1.521 (3) C11—C12 1.397 (2)
C24—C27 1.523 (3) C11—C16 1.398 (2)
C25—H25A 0.9800 C12—C13 1.392 (2)
C25—H25B 0.9800 C12—H12 0.9500
C25—H25C 0.9800 C13—C14 1.381 (3)
C26—H26A 0.9800 C13—H13 0.9500
C26—H26B 0.9800 C14—C15 1.386 (3)
C26—H26C 0.9800 C14—Cl1 1.7446 (18)
C27—H27A 0.9800 C15—C16 1.388 (3)
C27—H27B 0.9800 C15—H15 0.9500
C27—H27C 0.9800 C16—H16 0.9500
N1—C4 1.376 (2) C17—C22 1.383 (3)
N1—C1 1.382 (2) C17—C18 1.391 (3)
N2—C6 1.376 (2) C18—C19 1.392 (3)
N2—C9 1.376 (2) C18—H18 0.9500
C1—C10 1.391 (2) C19—C20 1.375 (3)
C1—C2 1.438 (2) C19—H19 0.9500
C2—C3 1.348 (2) C20—C21 1.370 (3)
C2—H2 0.9500 C20—Cl2 1.7513 (18)
C3—C4 1.443 (2) C21—C22 1.394 (3)
C3—H3 0.9500 C21—H21 0.9500
C4—C5 1.404 (2) C22—H22 0.9500
C5—C6 1.400 (2)
C23—Fe—C23i 180.0 N1—C4—C3 110.35 (15)
C23—Fe—N1i 89.88 (6) C5—C4—C3 124.23 (16)
C23i—Fe—N1i 90.12 (6) C6—C5—C4 123.44 (16)
C23—Fe—N1 90.12 (6) C6—C5—C11 117.22 (15)
C23i—Fe—N1 89.88 (6) C4—C5—C11 119.32 (15)
N1i—Fe—N1 180.00 (5) N2—C6—C5 126.17 (15)
C23—Fe—N2i 97.71 (6) N2—C6—C7 109.97 (15)
C23i—Fe—N2i 82.29 (6) C5—C6—C7 123.69 (16)
N1i—Fe—N2i 89.75 (6) C8—C7—C6 106.95 (16)
N1—Fe—N2i 90.25 (6) C8—C7—H7 126.5
C23—Fe—N2 82.29 (6) C6—C7—H7 126.5
C23i—Fe—N2 97.71 (6) C7—C8—C9 107.09 (16)
N1i—Fe—N2 90.25 (6) C7—C8—H8 126.5
N1—Fe—N2 89.75 (6) C9—C8—H8 126.5
N2i—Fe—N2 180.00 (4) N2—C9—C10i 125.90 (16)
N3—C23—Fe 165.75 (15) N2—C9—C8 110.34 (15)
C23—N3—C24 163.66 (17) C10i—C9—C8 123.75 (16)
N3—C24—C26 107.17 (15) C1—C10—C9i 124.00 (16)
N3—C24—C25 106.85 (15) C1—C10—C17 118.33 (15)
C26—C24—C25 110.81 (17) C9i—C10—C17 117.65 (15)
N3—C24—C27 109.23 (16) C12—C11—C16 118.18 (16)
C26—C24—C27 111.31 (17) C12—C11—C5 121.71 (16)
C25—C24—C27 111.25 (16) C16—C11—C5 120.05 (16)
C24—C25—H25A 109.5 C13—C12—C11 121.30 (17)
C24—C25—H25B 109.5 C13—C12—H12 119.4
H25A—C25—H25B 109.5 C11—C12—H12 119.4
C24—C25—H25C 109.5 C14—C13—C12 118.74 (17)
H25A—C25—H25C 109.5 C14—C13—H13 120.6
H25B—C25—H25C 109.5 C12—C13—H13 120.6
C24—C26—H26A 109.5 C13—C14—C15 121.51 (17)
C24—C26—H26B 109.5 C13—C14—Cl1 118.87 (14)
H26A—C26—H26B 109.5 C15—C14—Cl1 119.55 (14)
C24—C26—H26C 109.5 C14—C15—C16 118.98 (17)
H26A—C26—H26C 109.5 C14—C15—H15 120.5
H26B—C26—H26C 109.5 C16—C15—H15 120.5
C24—C27—H27A 109.5 C15—C16—C11 121.10 (17)
C24—C27—H27B 109.5 C15—C16—H16 119.4
H27A—C27—H27B 109.5 C11—C16—H16 119.4
C24—C27—H27C 109.5 C22—C17—C18 117.94 (17)
H27A—C27—H27C 109.5 C22—C17—C10 120.72 (16)
H27B—C27—H27C 109.5 C18—C17—C10 121.34 (16)
C4—N1—C1 105.33 (14) C17—C18—C19 121.09 (18)
C4—N1—Fe 127.86 (11) C17—C18—H18 119.5
C1—N1—Fe 126.77 (11) C19—C18—H18 119.5
C6—N2—C9 105.64 (14) C20—C19—C18 119.22 (18)
C6—N2—Fe 127.13 (11) C20—C19—H19 120.4
C9—N2—Fe 126.32 (11) C18—C19—H19 120.4
N1—C1—C10 125.79 (16) C21—C20—C19 121.22 (17)
N1—C1—C2 110.18 (15) C21—C20—Cl2 119.33 (16)
C10—C1—C2 123.93 (16) C19—C20—Cl2 119.44 (15)
C3—C2—C1 107.24 (16) C20—C21—C22 118.95 (19)
C3—C2—H2 126.4 C20—C21—H21 120.5
C1—C2—H2 126.4 C22—C21—H21 120.5
C2—C3—C4 106.85 (16) C17—C22—C21 121.57 (18)
C2—C3—H3 126.6 C17—C22—H22 119.2
C4—C3—H3 126.6 C21—C22—H22 119.2
N1—C4—C5 125.39 (16)