| Nonius Kappa APEXII diffractometer | 5201 independent reflections |
| Radiation source: X-ray tube | 4077 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.052 |
| Detector resolution: 512 x 512 pixels mm-1 | θmax = 27.5°, θmin = 2.4° |
| φ and ω scans | h = −14→14 |
| Absorption correction: numerical (SADABS; Krause et al., 2015) | k = −22→21 |
| Tmin = 0.903, Tmax = 0.982 | l = −17→15 |
| 44887 measured reflections |
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