| Agilent Xcalibur, Atlas, Gemini diffractometer | 1946 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.091 |
| ω scans | θmax = 28.5°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | h = −9→9 |
| Tmin = 0.631, Tmax = 0.746 | k = −13→13 |
| 68672 measured reflections | l = −27→27 |
| 3872 independent reflections |