Agilent Xcalibur, Atlas, Gemini diffractometer | 2853 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.038 |
ω scans | θmax = 28.7°, θmin = 2.4° |
Absorption correction: multi-scan | h = −11→11 |
Tmin = 0.819, Tmax = 0.937 | k = −18→18 |
45801 measured reflections | l = −14→14 |
3296 independent reflections |