Table 3.
Peak | RT (min) | ESI–MS | Identification | Bioactive compounds content (%) | ||
---|---|---|---|---|---|---|
Raw seed | DP pre-treatment (1.0 MPa) | WP pre-treatment (90 °C) | ||||
1 | 1.967 | 353 [M−H]− | Chlorogenic acid | 0.47 ± 0.04a | 0.41 ± 0.02b | 0.23 ± 0.005c |
2 | 2.808 | 595 [M+HCOO]− | Genipin-1-gentiobioside | 1.65 ± 0.07a | 1.54 ± 0.30a | 1.53 ± 0.008a |
3 | 3.343 | 433 [M+HCOO]− | Geniposide | 7.68 ± 0.06a | 6.86 ± 0.37b | 6.83 ± 0.05b |
4 | 5.438 | 609 [M−H]− | Rutin | 0.63 ± 0.13a | 0.57 ± 0.02b | 0.59 ± 0.002ab |
5 | 7.318 | 975 [M−H]− | Crocin | 10.45 ± 0.07a | 6.67 ± 0.06b | 9.20 ± 0.02c |
Values were the mean ± SD of three gardenia seed oils which was analyzed in triplicate. The average values in the same row followed by the same superior letters were not significantly different (p > 0.05)