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GC-MS/MS detection parameters
| Items | Parameters |
|---|---|
| Injection volume | 1 µL |
| Front Inlet Mode | 5:1 |
| Carrier Gas | Helium |
| Column | DB-FFAP (30m x 0.25mm x 0.25µm) |
| Column Flow | 1.2 mL/min |
| Oven Temperature Ramp | held at 50°C for 1 min, raised to 220°C at a rate of 18°C/min and kept for 5 min. |
| Front Injection Temperature | 250°C |
| Transfer Line Temperature | 230°C |
| Ion Source Temperature | 230°C |
| Quad Temperature | 150°C |
