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. 2023 Oct 13;9(10):e20967. doi: 10.1016/j.heliyon.2023.e20967

Table 2.

Experimental design (three levels–three variables) using a mixture of diluted acids as the extractant.

Experiment HNO3(mol L−1) HCl (mol L−1) Time (min) %R (Fe) %R (Mn)
1 0.7 0.6 10 82.5 108
2 0.7 0.6 20 81.5 113
3 1.4 1.2 15 83.6 114
4 2.25 2.0 10 78.9 102
5 2.25 2.0 15 70.2 105

%R: mean recovery percentage after analysis of the bovine muscle CRM (n = 6 replicates of each experiment) [31].