Table 2.
Experimental design (three levels–three variables) using a mixture of diluted acids as the extractant.
| Experiment | HNO3(mol L−1) | HCl (mol L−1) | Time (min) | %R (Fe) | %R (Mn) |
|---|---|---|---|---|---|
| 1 | 0.7 | 0.6 | 10 | 82.5 | 108 |
| 2 | 0.7 | 0.6 | 20 | 81.5 | 113 |
| 3 | 1.4 | 1.2 | 15 | 83.6 | 114 |
| 4 | 2.25 | 2.0 | 10 | 78.9 | 102 |
| 5 | 2.25 | 2.0 | 15 | 70.2 | 105 |
%R: mean recovery percentage after analysis of the bovine muscle CRM (n = 6 replicates of each experiment) [31].