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. Author manuscript; available in PMC: 2024 Oct 11.
Published in final edited form as: J Am Chem Soc. 2023 Oct 3;145(40):21738–21744. doi: 10.1021/jacs.3c08428

Table 3.

Alkene Scopea

graphic file with name nihms-1937179-t0005.jpg
a

Yields are the average of two experiments and are for isolated material on 0.5 mmol scale unless otherwise noted.

b

1.5 equiv. alkene.

c

2.5 equiv. alkene.

d

5.0 equiv. alkene.

e

PhCF3 solvent.

f

[Ir(dF(CF3)ppy)2(bpy)]OTf photocatalyst.

g

From the corresponding triisopropylsilyl enol ether.