Skip to main content
. 2023 Oct 9;13(20):13607–13617. doi: 10.1021/acscatal.3c03832

Table 1. Optimization of Reaction Conditions.

graphic file with name cs3c03832_0013.jpg

entry catalyst (mol %) 2 (equiv vs 1) yield (%)a
1 none 1 20
2 none 10 35
3 CoCl2 (5) 10 42
4 III (5) 1 18
5 III (5) 3 43
6 III (5) 5 58
7 III (5) 10 73
8 III (5) 20 73
9b none 10 0
10b III (5) 10 <1
11 III (5) 10 74
a

Yields were determined by integration of 19F NMR resonances using C6F6 as an internal standard based on 1 as the limiting reagent, as described in the Supporting Information.

b

Reaction performed in the dark.