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. 2023 Oct 31;14:6956. doi: 10.1038/s41467-023-42329-9

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© The Author(s) 2023

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 6 — a The top panel shows the weight fractions obtained for the target and its competing polymorph (o-LTOPO) based on each precursor set that was tested at 700 °C. The bottom panel displays the weight fraction of a common impurity phase, LiTi₂(PO₄)₃, obtained at 400 °C. Solid (hollow) dots represent experimental (predicted) values. b X-ray diffraction (XRD) pattern measured from the synthesis product of the optimized precursor set, Li₂O + TiO₂ + P₂O₅, which was ball milled and subsequently heated to 700 °C for 4 h. For comparison, a reference pattern for t-LTOPO (ICSD #39761) is also shown.