| Crystal data |
| Chemical formula |
C15H15NO2
|
|
M
r
|
241.28 |
| Crystal system, space group |
Monoclinic, P21/c
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
9.6678 (8), 10.9294 (11), 11.7231 (8) |
| β (°) |
93.395 (7) |
|
V (Å3) |
1236.53 (18) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.69 |
| Crystal size (mm) |
0.08 × 0.04 × 0.02 |
| |
| Data collection |
| Diffractometer |
SuperNova, Dual, Cu at zero, Eos |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2015 ▸) |
|
T
min, T
max
|
0.919, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
4437, 2285, 1828 |
|
R
int
|
0.019 |
| (sin θ/λ)max (Å−1) |
0.609 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.045, 0.131, 1.04 |
| No. of reflections |
2285 |
| No. of parameters |
166 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.25, −0.20 |
